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內(nèi)容簡介

　　本書是《農(nóng)藥獸藥多組分殘留質(zhì)譜分析技術(shù)》的第2卷獸藥篇，介紹了65項(xiàng)適用于動(dòng)物組織（肌肉、肝臟、腎臟和脂肪）、乳制品（牛奶和奶粉）、蜂產(chǎn)品（蜂蜜、蜂王漿及凍干粉）、水產(chǎn)品（河豚魚、鰻魚和烤鰻）及動(dòng)物尿液中20類獸藥殘留LC-MS/MS分析方法。方法靈敏度和準(zhǔn)確度高，可滿足歐盟、日本、國際食品法典委員會(huì)（CAC）和美國等限量要求。各章按獸藥類別，分別介紹了磺胺類、β-受體激動(dòng)劑類、氨基糖苷類、氯霉素類、β-內(nèi)酰胺類、大環(huán)內(nèi)酯類和林可胺類、硝基呋喃類代謝物、甾體類同化激素、非甾類同化激素類、糖皮質(zhì)激素類、氟喹諾酮類、四環(huán)素類、鎮(zhèn)靜劑類、吡唑酮類、喹啉類、硝基咪唑類、苯并咪唑類、咪唑并噻唑類、硫脲嘧啶類、聚醚類等20類獸藥的前處理技術(shù)和測(cè)定方法，并介紹了獸藥的理化性質(zhì)、代謝和毒理及大殘留限量等。本書可供從事食品安全、農(nóng)業(yè)環(huán)境保護(hù)及農(nóng)藥開發(fā)利用等技術(shù)研究與應(yīng)用的技術(shù)人員參考，也可作為大學(xué)教學(xué)參考用書。

作者簡介

　　龐國芳，中國檢驗(yàn)檢疫科學(xué)研究院，研究員，中國工程院院士，國家質(zhì)檢總局首席研究員、國際公職化學(xué)家聯(lián)合會(huì)（AOAC）專家，國際AOAC 2014年度 Harvey W. Wiley 獎(jiǎng)獲得者。近30年一直工作在食品檢驗(yàn)檢疫一線，致力于食品科學(xué)檢測(cè)技術(shù)理論與實(shí)踐的研究，解決了我國相關(guān)出口食品、農(nóng)產(chǎn)品等遭遇的技術(shù)瓶頸，為推動(dòng)我國對(duì)外貿(mào)易發(fā)展做出了杰出貢獻(xiàn)。研究制定了141項(xiàng)國際、國家檢測(cè)技術(shù)標(biāo)準(zhǔn)。在國內(nèi)、國際出版食品安全檢測(cè)技術(shù)論著10部。發(fā)表論文100余篇，35篇被SCI收錄。3次榮獲國家科學(xué)技術(shù)進(jìn)步二等獎(jiǎng)，6次榮獲國際AOAC組織頒發(fā)的科學(xué)技術(shù)獎(jiǎng)勵(lì)。

圖書目錄

Main Researchers/Editors xxvii
Preface xxix
Brief Introduction xxxi

1. Sulfonamides 1
1.1 Curative Effects and Side Effects of Sulfonamides 1
1.2 Chemical Structures and Maximum Residue Limits for Sulfonamide Drugs 2
1.3 Determination of 16 Sulfonamide Residues in Livestock and Poultry Muscles—LC-MS-MS Method (GB/T 20759-2006) 8
1.3.1 Scope 8
1.3.2 Principle 8
1.3.3 Reagents and Materials 8
1.3.4 Apparatus 9
1.3.5 Sample Pretreatment 9
1.3.6 Determination 9
1.3.7 Precision 10
1.3.8 Recovery 12
Researchers 12
Further Reading 16
1.4 Determination of 16 Sulfonamide Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22966-2008) 16
1.4.1 Scope 16
1.4.2 Principle 16
1.4.3 Reagents and Materials 17
1.4.4 Apparatus 17
1.4.5 Sample Pretreatment 18
1.4.6 Determination 18
1.4.7 Precision 19
1.4.8 Recovery 28
Researchers 28
1.5 Determination of 18 Sulfonamide Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22951-2008) 29
1.5.1 Scope 29
1.5.2 Principle 29
1.5.3 Reagents and Materials 29
1.5.4 Apparatus 30
1.5.5 Sample Pretreatment 31
1.5.6 Determination 31
1.5.7 Precision 35
1.5.8 Recovery 36
Researchers 40
1.6 Determination of 8 Sulfonamides residues in Honey—LC-FLD Method (GB/T 18932.5-2002) 41
1.6.1 Scope 41
1.6.2 Principle 41
1.6.3 Reagents and Materials 41
1.6.4 Apparatus 42
1.6.5 Sample Pretreatment 42
1.6.6 Determination 43
1.6.7 Precision 43
1.6.8 Recovery 46
Researchers 47
Further Reading 47
1.7 Determination of 16 Sulfonamide Residues in Honey—LC-MS-MS Method (GB/T 18932.17-2003) 47
1.7.1 Scope 47
1.7.2 Principle 47
1.7.3 Reagents and Materials 48
1.7.4 Apparatus 48
1.7.5 Sample Pretreatment 48
1.7.6 Determination 49
1.7.7 Precision 52
1.7.8 Recovery 52
Researchers 55
Further Reading 55
1.8 Determination of 18 Sulfonamide Residues in Royal Jelly—LC-MS-MS Method (GB/T 22947-2008) 56
1.8.1 Scope 56
1.8.2 Principle 56
1.8.3 Reagents and Materials 56
1.8.4 Apparatus 57
1.8.5 Sample Pretreatment 58
1.8.6 Determination 58
1.8.7 Precision 62
1.8.8 Recovery 64
Researchers 66

2. β-Adrenoceptor Agonists 67
2.1 Determination of 12 β-Agonist Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22965-2008) 67
2.1.1 Scope 67
2.1.2 Principle 67
2.1.3 Reagents and Materials 68
2.1.4 Apparatus 69
2.1.5 Sample Pretreatment 69
2.1.6 Determination 70
2.1.7 Precision 76
2.1.8 Recovery 76
Researchers 78
Further Reading 78
2.2 Determination of 12 β-Agonist Residues in Fugu, Eel,and Baked Eel—LC-MS-MS Method (GB/T 22950-2008) 81
2.2.1 Scope 81
2.2.2 Principle 81
2.2.3 Reagents and Materials 81
2.2.4 Apparatus 82
2.2.5 Sample Pretreatment 83
2.2.6 Determination 84
2.2.7 Precision 85
2.2.8 Recovery 85
Researchers 85
Further Reading 88

3. Aminoglycoside 91
3.1 Curative Effects and Side Effects of Streptomycin 91
3.2 Chemical Structures and Maximum Residue Limits for Streptomycin and Dihydrostreptomycin 92
3.3 Determination of Streptomycin Residues in Honey—LC-FLD (GB/T 18932.3-2002) 93
3.3.1 Scope 93
3.3.2 Principle 93
3.3.3 Reagents and Materials 93
3.3.4 Apparatus 94
3.3.5 Sample Pretreatment 95
3.3.6 Determination 95
3.3.7 Precision 97
3.3.8 Recovery 97
Researchers 97
Further Reading 97
3.4 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Milk and Milk
Powder—LC-MS-MS Method (GB/T 22969-2008) 98
3.4.1 Scope 98
3.4.2 Principle 98
3.4.3 Reagents and Materials 98
3.4.4 Apparatus 99
3.4.5 Preparation and Storage of Test Sample 100
3.4.6 Determination 101
3.4.7 Precision 104
3.4.8 Recovery 104
Researchers 105